Made In China Talk  

Go Back   Made In China Talk > International Business Talk > Import > Chemicals
Directory Register FAQ Members List Calendar Mark Forums Read 中文




how to remove hexane, how to solidify sticky oil?


Reply
 
Thread Tools Display Modes
  #1  
Old 04-10-2017, 11:16 PM
thomasmiller thomasmiller is offline
Junior Member
 
Join Date: Mar 2017
Posts: 20
Feedback: (0)
Default how to remove hexane, how to solidify sticky oil?

i separated just one spot, and then evaporated using rotary evaporater
in other reference my compound is white solid, but in my case sticky oil.
my compound is non-polar, and my compound is not soluble in diethyl ether, dichloromethane, ethyl acetate.
when i was soluble in that solvents, there is a little powder at the bottom of round flask.
but evaporating again my compound is sticky oil.
and i vacuumed 1 day and checked NMR. that NMR is not clear. hexane, water is remain.

Please Help.

Thanks !

I didn't find the right solution from the internet.
References:
-http://www.chemicalforums.com/index.php?topic=90837.0
-Web Video Pricing Examples
Reply With Quote




Reply



Thread Tools
Display Modes

Posting Rules
You may not post new threads
You may not post replies
You may not post attachments
You may not edit your posts

BB code is On
Smilies are On
[IMG] code is On
HTML code is Off
Forum Jump


| Business Forum | Toronto Chinese

All times are GMT +9. The time now is 08:49 PM.


All rights reserved. Copyright 2007 Made In China Talk